Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Wydział Technologii i Inżynierii Chemicznej - Inżynieria chemiczna (N3)

Sylabus przedmiotu Instrumental Analysis I:

Informacje podstawowe

Kierunek studiów Inżynieria chemiczna
Forma studiów studia niestacjonarne Poziom trzeciego stopnia
Stopnień naukowy absolwenta doktor
Obszary studiów studia trzeciego stopnia
Profil
Moduł
Przedmiot Instrumental Analysis I
Specjalność przedmiot wspólny
Jednostka prowadząca Instytut Technologii Chemicznej Nieorganicznej i Inżynierii Środowiska
Nauczyciel odpowiedzialny Mirosława El Fray <Miroslawa.ElFray@zut.edu.pl>
Inni nauczyciele Elżbieta Filipek <Elzbieta.Filipek@zut.edu.pl>, Zofia Lendzion-Bieluń <Zofia.Lendzion-Bielun@zut.edu.pl>, Dariusz Moszyński <Dariusz.Moszynski@zut.edu.pl>, Robert Pełech <Robert.Pelech@zut.edu.pl>, Agnieszka Piegat <Agnieszka.Piegat@zut.edu.pl>, Jacek Przepiórski <Jacek.Przepiorski@zut.edu.pl>, Zbigniew Rozwadowski <Zbigniew.Rozwadowski@zut.edu.pl>, Rafał Wróbel <Rafal.Wrobel@zut.edu.pl>
ECTS (planowane) 1,0 ECTS (formy) 1,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny Grupa obieralna

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
wykładyW1 8 1,01,00zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Fundamentals of chemical qualitative and quantitative analysis

Cele przedmiotu

KODCel modułu/przedmiotu
C-1To familiarize students with instrumental methods used in the study of properties of various materials
C-2Developing skills of selection of instrumental methods for determining the properties of characterized material

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
wykłady
T-W-1Magnetochemical methods of materials testing (types and classes of magnetic substances, properties, magnetic moment, effective magnetic moment, force method of determining the magnetic susceptibility, the use of magnetic measurements)1
T-W-2Introduction to spectroscopic techniques of surface analysis: Auger Electron Spectroscopy (AES) and X-ray Photoelectron Spectroscopy (XPS)1
T-W-3Use of NMR method in the structural studies (NMR spectrum of organic compounds, factors influencing the spectral parameters and their dependence on the structure of organic compounds, NMR 1D and 2D spectra used in structural studies, NMR of different nuclei, application of CP MAS NMR.1
T-W-4Selected chromatographic methods in the trace analysis (fundamentals and practical application of some chromatographic techniques used in the analysis of traces of volatile organic compounds: Purge & Trap, Direct Aqueous Injection/ Electron Capture Detector)1
T-W-5X-ray fluorescence analysis (the construction of the spectrometer, principle of formation of a secondary fluorescent radiation, method application, sample preparation, matrix effects).1
T-W-6Analysis of material with the combined TG-MS method (base thermogravimetry and mass spectrometry, the opportunities and benefits resulting from the merge of both techniques, sample measurement procedures and method application)1
T-W-7X-ray diffraction analysis - the basics of crystallography and diffraction (unit cell, crystallographic systems, lattice, spacing, the properties and formation of the X-ray radiation, X-ray tube construction, X-ray radiation counters)1
T-W-8Dynamic light scattering method as a technique for the determination of a particle size. The theory of dynamic light scattering in determining a particle size. Static light scattering, Rayleigh theory.1
8

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
wykłady
A-W-1participation in classes8
A-W-2to familiarize yourself with the issues given in a lecture on the basis of the given literature12
A-W-3preparation for the grade10
30

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1lecture
M-2consultations

Sposoby oceny

KODSposób oceny
S-1Ocena formująca: participation in lectures
S-2Ocena podsumowująca: completion of lectures

Zamierzone efekty kształcenia - wiedza

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla dyscyplinyOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChE_3-_B02_W01
Student knows the research methods used to determine the various properties of materials and explains the principle of operation used equipment
ChE_3-_W04C-1, C-2T-W-1, T-W-2, T-W-3, T-W-4, T-W-5, T-W-6, T-W-7, T-W-8M-1, M-2S-1, S-2

Zamierzone efekty kształcenia - umiejętności

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla dyscyplinyOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChE_3-_B02_U01
Student can suggest a suitable test method for determination of the properties of the materials and indicate the possibility of using the obtained results
ChE_3-_U08, ChE_3-_U10C-1, C-2T-W-1, T-W-2, T-W-3, T-W-4, T-W-5, T-W-6, T-W-7, T-W-8M-1, M-2S-1, S-2

Zamierzone efekty kształcenia - inne kompetencje społeczne i personalne

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla dyscyplinyOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChE_3-_B02_K01
Student is open to the knowledge improvement in the field of innovation and to transfer its skills to the others
ChE_3-_K01C-2T-W-1, T-W-2, T-W-3, T-W-4, T-W-5, T-W-6, T-W-7, T-W-8M-1, M-2S-1, S-2

Kryterium oceny - wiedza

Efekt kształceniaOcenaKryterium oceny
ChE_3-_B02_W01
Student knows the research methods used to determine the various properties of materials and explains the principle of operation used equipment
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student knows several research methods used to determine various properties of materials and partly explains the principle of operation of the apparatus used
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt kształceniaOcenaKryterium oceny
ChE_3-_B02_U01
Student can suggest a suitable test method for determination of the properties of the materials and indicate the possibility of using the obtained results
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student can suggest a suitable test method to determine the properties of materials
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt kształceniaOcenaKryterium oceny
ChE_3-_B02_K01
Student is open to the knowledge improvement in the field of innovation and to transfer its skills to the others
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student is open to a limited extent to the knowledge improvement in the field of innovation and to transfer its skills to the others
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. Chemia fizyczna, pr. zbiorowa, Rozdział 10.8 – Magnetyczne własności cząsteczek., PWN, Warszawa, 1980
  2. Galen W. Ewing, Metody instrumentalne w analizie chemicznej, PWN, Warszawa, 1980
  3. R.M. Silverstein, Spektroskopowe metody identyfikacji związków organicznych, PWN, Warszawa, 2012
  4. Praca zbiorowa, Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych, WNT, Warszawa, 2000
  5. Z. Witkiewicz, Podstawy chromatografii, WNT, Warszawa, 2000
  6. A. S. Płaziak, 2. A.S. Płaziak, Spektrometria masowa związków organicznych, Wydawnictwo Naukowe UAM, Poznań 1997., Wydawnictwo Naukowe UAM, Poznań, 1997
  7. B. Dziunikowski, Radiometryczne metody analizy chemicznej, WNT, Warszawa, 1991
  8. M. E. Brown, Introduction to Thermal Analysis. Techniques and Applications, Kluwer Academic Publishers, Dordrecht, 2001
  9. D. Senczyk, Polikrystaliczny dyfraktometr rentgenowski, Wydawnictwo Politechniki Poznańskiej, Poznań, 1999
  10. W. Bednarski, J. Fiedurek, Podstawy biotechnologii przemysłowej, WNT, Warszawa, 2007
  11. http://www.malvern.com/LabEng/products/zetasizer/zetasizer.htm, 2015

Literatura dodatkowa

  1. B.Staliński, Magnetochemia, PWN, Warszawa, 1966
  2. S. Berger, S. Braun, 200 and more basic NMR experiments, Wiley VCH, Weinheim, 2004
  3. E. Breitmaier, Structure elucidation by NMR in organic chemistry, Wiley, Chichester, 1993
  4. E. de Hoffmann, J. Charatte, V. Stroobant, Spektrometria mas, WNT, Warszawa, 1998
  5. Praca zbiorowa pod redakcją J. Ciby, Poradnik Chemika Analityka, Analiza instrumentalna, Tom 2, WNT, Warszawa, 1998
  6. Z. Bojarski, E. Łągiewka, Rentgenowska analiza strukturalna, Skrypt Uniwersytetu Śląskiego, Gliwice, 1995, 510
  7. K. Szewczyk, Technologia biochemiczna, Oficyna Wydawnicza Politechniki Warszawskiej, Warszawa, 2003

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1Magnetochemical methods of materials testing (types and classes of magnetic substances, properties, magnetic moment, effective magnetic moment, force method of determining the magnetic susceptibility, the use of magnetic measurements)1
T-W-2Introduction to spectroscopic techniques of surface analysis: Auger Electron Spectroscopy (AES) and X-ray Photoelectron Spectroscopy (XPS)1
T-W-3Use of NMR method in the structural studies (NMR spectrum of organic compounds, factors influencing the spectral parameters and their dependence on the structure of organic compounds, NMR 1D and 2D spectra used in structural studies, NMR of different nuclei, application of CP MAS NMR.1
T-W-4Selected chromatographic methods in the trace analysis (fundamentals and practical application of some chromatographic techniques used in the analysis of traces of volatile organic compounds: Purge & Trap, Direct Aqueous Injection/ Electron Capture Detector)1
T-W-5X-ray fluorescence analysis (the construction of the spectrometer, principle of formation of a secondary fluorescent radiation, method application, sample preparation, matrix effects).1
T-W-6Analysis of material with the combined TG-MS method (base thermogravimetry and mass spectrometry, the opportunities and benefits resulting from the merge of both techniques, sample measurement procedures and method application)1
T-W-7X-ray diffraction analysis - the basics of crystallography and diffraction (unit cell, crystallographic systems, lattice, spacing, the properties and formation of the X-ray radiation, X-ray tube construction, X-ray radiation counters)1
T-W-8Dynamic light scattering method as a technique for the determination of a particle size. The theory of dynamic light scattering in determining a particle size. Static light scattering, Rayleigh theory.1
8

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1participation in classes8
A-W-2to familiarize yourself with the issues given in a lecture on the basis of the given literature12
A-W-3preparation for the grade10
30
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaChE_3-_B02_W01Student knows the research methods used to determine the various properties of materials and explains the principle of operation used equipment
Odniesienie do efektów kształcenia dla dyscyplinyChE_3-_W04She/he has advanced knowledge of techniques and methods to identify and characterize chemical products.
Cel przedmiotuC-1To familiarize students with instrumental methods used in the study of properties of various materials
C-2Developing skills of selection of instrumental methods for determining the properties of characterized material
Treści programoweT-W-1Magnetochemical methods of materials testing (types and classes of magnetic substances, properties, magnetic moment, effective magnetic moment, force method of determining the magnetic susceptibility, the use of magnetic measurements)
T-W-2Introduction to spectroscopic techniques of surface analysis: Auger Electron Spectroscopy (AES) and X-ray Photoelectron Spectroscopy (XPS)
T-W-3Use of NMR method in the structural studies (NMR spectrum of organic compounds, factors influencing the spectral parameters and their dependence on the structure of organic compounds, NMR 1D and 2D spectra used in structural studies, NMR of different nuclei, application of CP MAS NMR.
T-W-4Selected chromatographic methods in the trace analysis (fundamentals and practical application of some chromatographic techniques used in the analysis of traces of volatile organic compounds: Purge & Trap, Direct Aqueous Injection/ Electron Capture Detector)
T-W-5X-ray fluorescence analysis (the construction of the spectrometer, principle of formation of a secondary fluorescent radiation, method application, sample preparation, matrix effects).
T-W-6Analysis of material with the combined TG-MS method (base thermogravimetry and mass spectrometry, the opportunities and benefits resulting from the merge of both techniques, sample measurement procedures and method application)
T-W-7X-ray diffraction analysis - the basics of crystallography and diffraction (unit cell, crystallographic systems, lattice, spacing, the properties and formation of the X-ray radiation, X-ray tube construction, X-ray radiation counters)
T-W-8Dynamic light scattering method as a technique for the determination of a particle size. The theory of dynamic light scattering in determining a particle size. Static light scattering, Rayleigh theory.
Metody nauczaniaM-1lecture
M-2consultations
Sposób ocenyS-1Ocena formująca: participation in lectures
S-2Ocena podsumowująca: completion of lectures
Kryteria ocenyOcenaKryterium oceny
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student knows several research methods used to determine various properties of materials and partly explains the principle of operation of the apparatus used
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaChE_3-_B02_U01Student can suggest a suitable test method for determination of the properties of the materials and indicate the possibility of using the obtained results
Odniesienie do efektów kształcenia dla dyscyplinyChE_3-_U08She/he is able to use analytical methods and experimental research to solve problems in the field of chemical technology or chemical engineering, especially in terms of the direction of research.
ChE_3-_U10She/he is able to assess the usefulness and ability to use new technological studies and research methods in terms of the direction of research.
Cel przedmiotuC-1To familiarize students with instrumental methods used in the study of properties of various materials
C-2Developing skills of selection of instrumental methods for determining the properties of characterized material
Treści programoweT-W-1Magnetochemical methods of materials testing (types and classes of magnetic substances, properties, magnetic moment, effective magnetic moment, force method of determining the magnetic susceptibility, the use of magnetic measurements)
T-W-2Introduction to spectroscopic techniques of surface analysis: Auger Electron Spectroscopy (AES) and X-ray Photoelectron Spectroscopy (XPS)
T-W-3Use of NMR method in the structural studies (NMR spectrum of organic compounds, factors influencing the spectral parameters and their dependence on the structure of organic compounds, NMR 1D and 2D spectra used in structural studies, NMR of different nuclei, application of CP MAS NMR.
T-W-4Selected chromatographic methods in the trace analysis (fundamentals and practical application of some chromatographic techniques used in the analysis of traces of volatile organic compounds: Purge & Trap, Direct Aqueous Injection/ Electron Capture Detector)
T-W-5X-ray fluorescence analysis (the construction of the spectrometer, principle of formation of a secondary fluorescent radiation, method application, sample preparation, matrix effects).
T-W-6Analysis of material with the combined TG-MS method (base thermogravimetry and mass spectrometry, the opportunities and benefits resulting from the merge of both techniques, sample measurement procedures and method application)
T-W-7X-ray diffraction analysis - the basics of crystallography and diffraction (unit cell, crystallographic systems, lattice, spacing, the properties and formation of the X-ray radiation, X-ray tube construction, X-ray radiation counters)
T-W-8Dynamic light scattering method as a technique for the determination of a particle size. The theory of dynamic light scattering in determining a particle size. Static light scattering, Rayleigh theory.
Metody nauczaniaM-1lecture
M-2consultations
Sposób ocenyS-1Ocena formująca: participation in lectures
S-2Ocena podsumowująca: completion of lectures
Kryteria ocenyOcenaKryterium oceny
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student can suggest a suitable test method to determine the properties of materials
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaChE_3-_B02_K01Student is open to the knowledge improvement in the field of innovation and to transfer its skills to the others
Odniesienie do efektów kształcenia dla dyscyplinyChE_3-_K01She/he is able to think and act in an innovative, creative and enterprising way.
Cel przedmiotuC-2Developing skills of selection of instrumental methods for determining the properties of characterized material
Treści programoweT-W-1Magnetochemical methods of materials testing (types and classes of magnetic substances, properties, magnetic moment, effective magnetic moment, force method of determining the magnetic susceptibility, the use of magnetic measurements)
T-W-2Introduction to spectroscopic techniques of surface analysis: Auger Electron Spectroscopy (AES) and X-ray Photoelectron Spectroscopy (XPS)
T-W-3Use of NMR method in the structural studies (NMR spectrum of organic compounds, factors influencing the spectral parameters and their dependence on the structure of organic compounds, NMR 1D and 2D spectra used in structural studies, NMR of different nuclei, application of CP MAS NMR.
T-W-4Selected chromatographic methods in the trace analysis (fundamentals and practical application of some chromatographic techniques used in the analysis of traces of volatile organic compounds: Purge & Trap, Direct Aqueous Injection/ Electron Capture Detector)
T-W-5X-ray fluorescence analysis (the construction of the spectrometer, principle of formation of a secondary fluorescent radiation, method application, sample preparation, matrix effects).
T-W-6Analysis of material with the combined TG-MS method (base thermogravimetry and mass spectrometry, the opportunities and benefits resulting from the merge of both techniques, sample measurement procedures and method application)
T-W-7X-ray diffraction analysis - the basics of crystallography and diffraction (unit cell, crystallographic systems, lattice, spacing, the properties and formation of the X-ray radiation, X-ray tube construction, X-ray radiation counters)
T-W-8Dynamic light scattering method as a technique for the determination of a particle size. The theory of dynamic light scattering in determining a particle size. Static light scattering, Rayleigh theory.
Metody nauczaniaM-1lecture
M-2consultations
Sposób ocenyS-1Ocena formująca: participation in lectures
S-2Ocena podsumowująca: completion of lectures
Kryteria ocenyOcenaKryterium oceny
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student is open to a limited extent to the knowledge improvement in the field of innovation and to transfer its skills to the others
3,5
4,0
4,5
5,0