Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Administracja Centralna Uczelni - Wymiana międzynarodowa (S2)

Sylabus przedmiotu Fundamentals of crystallography and diffraction methods:

Informacje podstawowe

Kierunek studiów Wymiana międzynarodowa
Forma studiów studia stacjonarne Poziom drugiego stopnia
Tytuł zawodowy absolwenta
Obszary studiów
Profil
Moduł
Przedmiot Fundamentals of crystallography and diffraction methods
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Chemii Nieorganicznej i Analitycznej
Nauczyciel odpowiedzialny Piotr Tabero <Piotr.Tabero@zut.edu.pl>
Inni nauczyciele Monika Bosacka <Monika.Bosacka@zut.edu.pl>, Anna Błońska-Tabero <Anna.Blonska-Tabero@zut.edu.pl>, Grażyna Dąbrowska <Grazyna.Dabrowska@zut.edu.pl>, Elżbieta Filipek <Elzbieta.Filipek@zut.edu.pl>, Piotr Tabero <Piotr.Tabero@zut.edu.pl>, Elżbieta Tomaszewicz <Elzbieta.Tomaszewicz@zut.edu.pl>
ECTS (planowane) 4,0 ECTS (formy) 4,0
Forma zaliczenia zaliczenie Język polski
Blok obieralny Grupa obieralna

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
wykładyW2 30 2,00,50zaliczenie
ćwiczenia audytoryjneA2 30 2,00,50zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Fundamentals of mathematics, physics and chemistry

Cele przedmiotu

KODCel modułu/przedmiotu
C-1To acquaint students with the fundamentals of crystallography
C-2To acquaint students with methods of generation and properties of X-rays
C-3To acquaint students with the measuring techniques using diffraction phenomenon and their practical applications
C-4To teach students how to use stuctural data gained from diffraction measurements, available structural datebases and literature.

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
ćwiczenia audytoryjne
T-A-1Definition of crystalline body. Sructure of ideal solid. Morphology of crystals. Analysis and description of real objects: crystal, single crystal, twinns, intergrowths of crystals, policrystalline substance, amorphous substance, sand, gravel, silt, rock, mineral and solid.2
T-A-2Atomic and ionic radii. Coordination polyhedra. Connection of polyhedra. Crystal systems. Simple structures of elements and compounds: SC, BCC, FCC and HCP lattices.2
T-A-3Symmetry in crystals.Point groups and space groups. International Tables for Crystallograhy.2
T-A-4Structure and properties of solids. Cleavage, hardness. Defects in crystal structure. Solid solutions, their properties and application.2
T-A-5Generation and properties of of X-rays. Interaction of X-Rays with matter. Diffraction grating. X-ray diffraction on crystals.2
T-A-6Laue equation and Bragg equation. Intensity of diffraction reflections. Powder X-ray diffraction (PXRD). Preparation of samples for PXRD investigtions. Energy dispersive X-ray diffraction (EDXRD).2
T-A-7Preferred orientation of crystallites. Qualitative X-ray phase analysis. Identification of metals and alloys. Identification of minerals and components of rocks and sands from different locations.4
T-A-8Indexation of powder diffracion patterns. Lattice parameter determination. Measurement of density. Rentgenographic density.4
T-A-9Determination of grain size, internal stress and lattice distortions. Quanntitative X-Ray phase analysis.2
T-A-10X-ray high-temperature measurements. Determination of coefficients of thermal expansion. Anisotropy of thermal expansion. Investigations of plymorphic phase transitions.2
T-A-11Nanocrystalline, semicrystalline and amorphous materials- properties and investigation. Liquid crystals. Mesoporous molecular sieves.2
T-A-12Structure solution from powder diffraction. Rietveld refinement. Structure solution from single crystals. Diffraction of electrons and neutrons.4
30
wykłady
T-W-1Early historical notes. Basic definitions in crystallography. Solids. Physical properties of solids. Structure of "ideal" solid. Morphology of crystals.2
T-W-2Crystal systems and Bravais lattices. Symmetry in crystals. Point groups and space groups. International Tables for Crystallography2
T-W-3Atomic and ionic radii. Coordination polyhedra. Simple structures of elements and compounds: SC, BCC , FCC and HCP lattices.2
T-W-4Structure and properties of solids. Defect in crystal structure. Solid solutions.2
T-W-5Generation and properties of X-rays. Interaction of X-rays with matte. Safety procedures for x-ray equipment. X-ray diffraction on solids.2
T-W-6Laue equation and Bragg Law. Intensity of diffraction reflections.2
T-W-7Powder X-ray diffraction (PXRD). Energy-dispersive X-ray diffraction (EDXRD). Single crystal X-ray diffraction.2
T-W-8Qualitative XRD phase analysis. Preferred orientation of crystallites. X-ray techniques for texture investigations.2
T-W-9Quantitative X-ray phase analysis. Measurements of thickness of thin layers.2
T-W-10Lattice defects and diffraction pattern. Investigation of size of crystallites , internal stresses and lattice distortions. Rentgenographic density.2
T-W-11High-temperature , low-temperature and high-pressure XRD measurements. Investigation of polimorphic phase transitions and thermal expansion.2
T-W-12Nanocrystalline, semicrystalline and amorphous materials. Liquid crystals. Mesoporous molecular sieves.1
T-W-13Indexation of powder diffraction patterns. Precise determination of the unit cell parameters.2
T-W-14Structure solution from single crystals. Structure solution from powder patterns. Rietveld refinement.2
T-W-15XRD vs neutron and electron diffraction1
T-W-16The final written test2
30

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
ćwiczenia audytoryjne
A-A-1Participation in workshop30
A-A-2Participation in consultations2
A-A-3Self-study of literature12
A-A-4Preparation of written reports16
60
wykłady
A-W-1Participation in lectures30
A-W-2Participation in consultations2
A-W-3Self-study of literature12
A-W-4Preparing to pass written test based on the indicated literature and other sources of knowledge14
A-W-5Finnal written exam2
60

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1Informative lectures with multimedia instruments, explanation
M-2Work with computers and dedicated software

Sposoby oceny

KODSposób oceny
S-1Ocena podsumowująca: Final written exam
S-2Ocena podsumowująca: written reports

Zamierzone efekty kształcenia - wiedza

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_null_W01
Student knows fundamental concepts in crystallography and knows measuring techniques using diffraction phenomenon
C-1, C-2, C-3M-1S-1

Zamierzone efekty kształcenia - umiejętności

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_null_U01
Students is able to select appropriate diffraction measuring technique to investigate given property of material and interpret obtained results of investigation
C-1, C-2, C-3M-1S-1

Zamierzone efekty kształcenia - inne kompetencje społeczne i personalne

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_null_K01
Student knows safety procedures for x-ray equipment and understands importance of permanent learning to improve personal competencies
C-1, C-2, C-3M-1S-1

Kryterium oceny - wiedza

Efekt kształceniaOcenaKryterium oceny
WM-WTiICh_2-_null_W01
Student knows fundamental concepts in crystallography and knows measuring techniques using diffraction phenomenon
2,0
3,0Student will be able to present basic concepts of crystallography and describe basic measuring methods applying X-ray diffraction.
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt kształceniaOcenaKryterium oceny
WM-WTiICh_2-_null_U01
Students is able to select appropriate diffraction measuring technique to investigate given property of material and interpret obtained results of investigation
2,0
3,0Student will be able to select approprate XRD measuring technique to solve simple problem concerning analysis of crystalline solid
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt kształceniaOcenaKryterium oceny
WM-WTiICh_2-_null_K01
Student knows safety procedures for x-ray equipment and understands importance of permanent learning to improve personal competencies
2,0
3,0Student knows and understands safety procedures for x-ray equipment
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. C. Giacovazzo, H. Z. Monaco, D. Biterbo, F. Scordari, G. Gilli, G. Zanotti, M. Catti, Fundamentals of Crystallography, IUCR, Oxford University Press, Oxford, 2000
  2. D. B. Williams, C. B. Carter, Transmission Electron Microscopy, Plenum Press, New York and London, 1996
  3. O. Engler, V. Randle, Introduction to Texture Analysis. Macrotexture, Microtexture and Orientation Mapping, CRC Press, Taylor & Francis Group, London, New York, 2010
  4. Cullity B.D., Elements of X-ray Diffraction, Addison-Wesley Publishing Company, Inc., London, 1978
  5. P. Luger, Modern X-ray Analysis on Single Crystals, Walter de Gruyter and Co., Berlin, 1980
  6. Glusker, J. P.; Lewis, M.; Rossi, M., “Crystal Structure Analysis for Chemists and Biologists, VCH, New York, 1994
  7. W.I.F. David, K. Shankland, L.B. McCusker and Ch. Baerlocher, Edt., Structure determination form powder diffraction data. IUCr Monographs on crystallography, Oxford Science Publications, Oxford, 2002
  8. A. Gaunier, X-ray Diffraction in Crystals, Imperfect Crystals, and Amorphous Bodies, Courier Corporation, New York, 1994
  9. A. AUTHIER, G. CHAPUIS, EDS, A LITTLE DICTIONARY OF CRYSTALLOGRAPHY, INTERNATIONAL UNION OF CRYSTALLOGRAPHY, 2017, 2ND EDITION
  10. P. P. Ewald, Ed., Fifty Years of X-ray Diffraction, Reprinted in pdf format for the IUCr XVIII Congress, Glasgow, Scotland, Copyright © 1962, 1999 International Union of Crystallography, https://www.iucr.org

Literatura dodatkowa

  1. International Union of Crystallography: https://www.iucr.org
  2. http://www.xtal.iqfr.csic.es/Cristalografia/parte_01_1-en.html

Treści programowe - ćwiczenia audytoryjne

KODTreść programowaGodziny
T-A-1Definition of crystalline body. Sructure of ideal solid. Morphology of crystals. Analysis and description of real objects: crystal, single crystal, twinns, intergrowths of crystals, policrystalline substance, amorphous substance, sand, gravel, silt, rock, mineral and solid.2
T-A-2Atomic and ionic radii. Coordination polyhedra. Connection of polyhedra. Crystal systems. Simple structures of elements and compounds: SC, BCC, FCC and HCP lattices.2
T-A-3Symmetry in crystals.Point groups and space groups. International Tables for Crystallograhy.2
T-A-4Structure and properties of solids. Cleavage, hardness. Defects in crystal structure. Solid solutions, their properties and application.2
T-A-5Generation and properties of of X-rays. Interaction of X-Rays with matter. Diffraction grating. X-ray diffraction on crystals.2
T-A-6Laue equation and Bragg equation. Intensity of diffraction reflections. Powder X-ray diffraction (PXRD). Preparation of samples for PXRD investigtions. Energy dispersive X-ray diffraction (EDXRD).2
T-A-7Preferred orientation of crystallites. Qualitative X-ray phase analysis. Identification of metals and alloys. Identification of minerals and components of rocks and sands from different locations.4
T-A-8Indexation of powder diffracion patterns. Lattice parameter determination. Measurement of density. Rentgenographic density.4
T-A-9Determination of grain size, internal stress and lattice distortions. Quanntitative X-Ray phase analysis.2
T-A-10X-ray high-temperature measurements. Determination of coefficients of thermal expansion. Anisotropy of thermal expansion. Investigations of plymorphic phase transitions.2
T-A-11Nanocrystalline, semicrystalline and amorphous materials- properties and investigation. Liquid crystals. Mesoporous molecular sieves.2
T-A-12Structure solution from powder diffraction. Rietveld refinement. Structure solution from single crystals. Diffraction of electrons and neutrons.4
30

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1Early historical notes. Basic definitions in crystallography. Solids. Physical properties of solids. Structure of "ideal" solid. Morphology of crystals.2
T-W-2Crystal systems and Bravais lattices. Symmetry in crystals. Point groups and space groups. International Tables for Crystallography2
T-W-3Atomic and ionic radii. Coordination polyhedra. Simple structures of elements and compounds: SC, BCC , FCC and HCP lattices.2
T-W-4Structure and properties of solids. Defect in crystal structure. Solid solutions.2
T-W-5Generation and properties of X-rays. Interaction of X-rays with matte. Safety procedures for x-ray equipment. X-ray diffraction on solids.2
T-W-6Laue equation and Bragg Law. Intensity of diffraction reflections.2
T-W-7Powder X-ray diffraction (PXRD). Energy-dispersive X-ray diffraction (EDXRD). Single crystal X-ray diffraction.2
T-W-8Qualitative XRD phase analysis. Preferred orientation of crystallites. X-ray techniques for texture investigations.2
T-W-9Quantitative X-ray phase analysis. Measurements of thickness of thin layers.2
T-W-10Lattice defects and diffraction pattern. Investigation of size of crystallites , internal stresses and lattice distortions. Rentgenographic density.2
T-W-11High-temperature , low-temperature and high-pressure XRD measurements. Investigation of polimorphic phase transitions and thermal expansion.2
T-W-12Nanocrystalline, semicrystalline and amorphous materials. Liquid crystals. Mesoporous molecular sieves.1
T-W-13Indexation of powder diffraction patterns. Precise determination of the unit cell parameters.2
T-W-14Structure solution from single crystals. Structure solution from powder patterns. Rietveld refinement.2
T-W-15XRD vs neutron and electron diffraction1
T-W-16The final written test2
30

Formy aktywności - ćwiczenia audytoryjne

KODForma aktywnościGodziny
A-A-1Participation in workshop30
A-A-2Participation in consultations2
A-A-3Self-study of literature12
A-A-4Preparation of written reports16
60
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1Participation in lectures30
A-W-2Participation in consultations2
A-W-3Self-study of literature12
A-W-4Preparing to pass written test based on the indicated literature and other sources of knowledge14
A-W-5Finnal written exam2
60
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_null_W01Student knows fundamental concepts in crystallography and knows measuring techniques using diffraction phenomenon
Cel przedmiotuC-1To acquaint students with the fundamentals of crystallography
C-2To acquaint students with methods of generation and properties of X-rays
C-3To acquaint students with the measuring techniques using diffraction phenomenon and their practical applications
Metody nauczaniaM-1Informative lectures with multimedia instruments, explanation
Sposób ocenyS-1Ocena podsumowująca: Final written exam
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student will be able to present basic concepts of crystallography and describe basic measuring methods applying X-ray diffraction.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_null_U01Students is able to select appropriate diffraction measuring technique to investigate given property of material and interpret obtained results of investigation
Cel przedmiotuC-1To acquaint students with the fundamentals of crystallography
C-2To acquaint students with methods of generation and properties of X-rays
C-3To acquaint students with the measuring techniques using diffraction phenomenon and their practical applications
Metody nauczaniaM-1Informative lectures with multimedia instruments, explanation
Sposób ocenyS-1Ocena podsumowująca: Final written exam
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student will be able to select approprate XRD measuring technique to solve simple problem concerning analysis of crystalline solid
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_null_K01Student knows safety procedures for x-ray equipment and understands importance of permanent learning to improve personal competencies
Cel przedmiotuC-1To acquaint students with the fundamentals of crystallography
C-2To acquaint students with methods of generation and properties of X-rays
C-3To acquaint students with the measuring techniques using diffraction phenomenon and their practical applications
Metody nauczaniaM-1Informative lectures with multimedia instruments, explanation
Sposób ocenyS-1Ocena podsumowująca: Final written exam
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student knows and understands safety procedures for x-ray equipment
3,5
4,0
4,5
5,0