Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Wydział Technologii i Inżynierii Chemicznej - Inżynieria chemiczna (N3)

Sylabus przedmiotu Instrumental Analysis II:

Informacje podstawowe

Kierunek studiów Inżynieria chemiczna
Forma studiów studia niestacjonarne Poziom trzeciego stopnia
Stopnień naukowy absolwenta doktor inżynier
Obszary studiów studia trzeciego stopnia
Profil
Moduł
Przedmiot Instrumental Analysis II
Specjalność przedmiot wspólny
Jednostka prowadząca Instytut Technologii Chemicznej Nieorganicznej i Inżynierii Środowiska
Nauczyciel odpowiedzialny Mirosława El Fray <Miroslawa.ElFray@zut.edu.pl>
Inni nauczyciele Monika Bosacka <Monika.Bosacka@zut.edu.pl>, Zofia Lendzion-Bieluń <Zofia.Lendzion-Bielun@zut.edu.pl>, Dariusz Moszyński <Dariusz.Moszynski@zut.edu.pl>, Robert Pełech <Robert.Pelech@zut.edu.pl>, Agnieszka Piegat <Agnieszka.Piegat@zut.edu.pl>, Jacek Przepiórski <Jacek.Przepiorski@zut.edu.pl>, Zbigniew Rozwadowski <Zbigniew.Rozwadowski@zut.edu.pl>, Rafał Wróbel <Rafal.Wrobel@zut.edu.pl>
ECTS (planowane) 3,0 ECTS (formy) 3,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny Grupa obieralna

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
laboratoriaL2 24 3,01,00zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Completion of lectures of instrumental analysis

Cele przedmiotu

KODCel modułu/przedmiotu
C-1To familiarize students with instrumental methods used in the study of properties of various material
C-2Developing skills of selection of instrumental methods for determining the properties of characterized material
C-3Developing skills to develop research results, their interpretation and use in the characterization of materials

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
laboratoria
T-L-1Use of magnetochemical methods in the study of substances, such as: qualitative evaluation of magnetic properties, determination of the electronic structure of the central ion3
T-L-2The use of spectroscopic techniques in the analysis of the surface - study of the chemical composition of the surface materials by XPS3
T-L-3NMR methods used in the studies of organic compounds (preparation of the samples for measurement, the identification of selected compounds on the basis of a series of spectra 1D (1H, 13C, NOE) and 2D (HMQC, HMBC, COSY, NOESY)3
T-L-4The use of chromatographic methods in the trace analysis (refering to the analytical system GC/MS, and the system capabilities in qualitative and quantitative analysis on the example of the analysis of petrochemical products, selection of analysis conditions, use a library of mass spectra to identify the analytes)3
T-L-5Using x-ray fluorescence spectrometry methods for the analysis of the chemical composition of the materials, such as: determination of promoters (CaO, Al2O3), iron catalyst by standard addition method3
T-L-6The use of TG-MS method to the analysis of materials, for example decomposition of the mixture NH4HCO3 and CaCO33
T-L-7The use of X-ray diffraction studies of solids (construction and operation of X-ray diffractometer, qualitative and quantitative analysis of phase composition, determination of medium-sized crystallites and grains of the materials3
T-L-8Determining the particle size with DLS technique3
24

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
laboratoria
A-L-1participation in classes24
A-L-2preparation to the laboratory unit14
A-L-3preparation to the laboratory unit8
A-L-4preparation for the grade14
60

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1laboratory
M-2consultations

Sposoby oceny

KODSposób oceny
S-1Ocena formująca: participation in laboratories
S-2Ocena formująca: performing the report
S-3Ocena formująca: written grade
S-4Ocena podsumowująca: the average of the credits of each laboratory

Zamierzone efekty kształcenia - wiedza

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla dyscyplinyOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChE_3-_B04_W01
Student knows the research methods used to determine the various properties of materials and explains the principle of operation used equipment
C-1, C-2, C-3T-L-1, T-L-2, T-L-3, T-L-4, T-L-5, T-L-6, T-L-7, T-L-8M-1, M-2S-1, S-2, S-3
ChE_3-_B04_W02
Student knows the research methods used to determine the various properties of materials and explains the principle of operation used equipment
ChE_3-_W04C-2M-2

Zamierzone efekty kształcenia - umiejętności

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla dyscyplinyOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChE_3-_B04_U01
Student can suggest a suitable test method for determination of the properties of the materials and indicate the possibility of using the obtained results
ChE_3-_U10, ChE_3-_U08C-2, C-3T-L-1, T-L-2, T-L-3, T-L-4, T-L-5, T-L-6, T-L-7, T-L-8M-1, M-2S-1, S-2, S-3

Zamierzone efekty kształcenia - inne kompetencje społeczne i personalne

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla dyscyplinyOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChE_3-_B04_K01
Student is open to the knowledge improvement in the field of innovation and to transfer its skills to the others
ChE_3-_K01C-1, C-2, C-3T-L-1, T-L-2, T-L-3, T-L-4, T-L-5, T-L-6, T-L-7, T-L-8M-1, M-2S-1, S-2, S-3

Kryterium oceny - wiedza

Efekt kształceniaOcenaKryterium oceny
ChE_3-_B04_W01
Student knows the research methods used to determine the various properties of materials and explains the principle of operation used equipment
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student knows several research methods used to determine various properties of materials and partly explains the principle of operation of the apparatus
3,5
4,0
4,5
5,0
ChE_3-_B04_W02
Student knows the research methods used to determine the various properties of materials and explains the principle of operation used equipment
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student knows several research methods used to determine various properties of materials and partly explains the principle of operation of the apparatus used
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt kształceniaOcenaKryterium oceny
ChE_3-_B04_U01
Student can suggest a suitable test method for determination of the properties of the materials and indicate the possibility of using the obtained results
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student can suggest a suitable test method to determine the properties of materials
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt kształceniaOcenaKryterium oceny
ChE_3-_B04_K01
Student is open to the knowledge improvement in the field of innovation and to transfer its skills to the others
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student is open to a limited extent to the knowledge improvement in the field of innovation and to transfer its skills to the others
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. Chemia fizyczna, pr. zbiorowa, Rozdział 10.8 – Magnetyczne własności cząsteczek., PWN, Warszawa, 1980
  2. Galen W. Ewing, Metody instrumentalne w analizie chemicznej, PWN, Warszawa, 1980
  3. R.M. Silverstein, Spektroskopowe metody identyfikacji związków organicznych, PWN, Warszawa, 2012
  4. Praca zbiorowa, Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych, WNT, Warszawa, 2000
  5. Z. Witkiewicz, Podstawy chromatografii, WNT, Warszawa, 2000
  6. A. S. Płaziak, Spektrometria masowa związków organicznych, Wydawnictwo Naukowe UAM, Poznań 1997., Poznań, 1997
  7. B. Dziunikowski, Radiometryczne metody analizy chemicznej, WNT, Warszawa, 1991
  8. M. E. Brown, Introduction to Thermal Analysis. Techniques and Applications, Kluwer Academic Publishers, Dordrecht, 2001
  9. D. Senczyk, Polikrystaliczny dyfraktometr rentgenowski, Wydawnictwo Politechniki Poznańskiej, Poznań, 1999
  10. W. Bednarski, J. Fiedurek, Podstawy biotechnologii przemysłowej, WNT, Warszawa, 2007
  11. http://www.malvern.com/LabEng/products/zetasizer/zetasizer.htm, 2015

Literatura dodatkowa

  1. B. Staliński, Magnetochemia, PWN, Warszawa, 1966
  2. S. Berger, S. Braun, 200 and more basic NMR experiments, Wiley VCH, Weinheim, 2004
  3. E. Breitmaier, Structure elucidation by NMR in organic chemistry, Wiley, Chichester, 1993
  4. E. de Hoffmann, J. Charatte, V. Stroobant, Spektrometria mas, WNT, Warszawa, 1998
  5. Praca zbiorowa pod redakcją J. Ciby, Poradnik Chemika Analityka, Analiza instrumentalna, Tom 2, WNT, Warszawa, 1998
  6. Z. Bojarski, E. Łągiewka, Rentgenowska analiza strukturalna, Skrypt Uniwersytetu Śląskiego, Gliwice, 1995, 510
  7. K. Szewczyk, Technologia biochemiczna, Oficyna Wydawnicza Politechniki Warszawskiej, Warszawa, 2003

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Use of magnetochemical methods in the study of substances, such as: qualitative evaluation of magnetic properties, determination of the electronic structure of the central ion3
T-L-2The use of spectroscopic techniques in the analysis of the surface - study of the chemical composition of the surface materials by XPS3
T-L-3NMR methods used in the studies of organic compounds (preparation of the samples for measurement, the identification of selected compounds on the basis of a series of spectra 1D (1H, 13C, NOE) and 2D (HMQC, HMBC, COSY, NOESY)3
T-L-4The use of chromatographic methods in the trace analysis (refering to the analytical system GC/MS, and the system capabilities in qualitative and quantitative analysis on the example of the analysis of petrochemical products, selection of analysis conditions, use a library of mass spectra to identify the analytes)3
T-L-5Using x-ray fluorescence spectrometry methods for the analysis of the chemical composition of the materials, such as: determination of promoters (CaO, Al2O3), iron catalyst by standard addition method3
T-L-6The use of TG-MS method to the analysis of materials, for example decomposition of the mixture NH4HCO3 and CaCO33
T-L-7The use of X-ray diffraction studies of solids (construction and operation of X-ray diffractometer, qualitative and quantitative analysis of phase composition, determination of medium-sized crystallites and grains of the materials3
T-L-8Determining the particle size with DLS technique3
24

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1participation in classes24
A-L-2preparation to the laboratory unit14
A-L-3preparation to the laboratory unit8
A-L-4preparation for the grade14
60
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaChE_3-_B04_W01Student knows the research methods used to determine the various properties of materials and explains the principle of operation used equipment
Cel przedmiotuC-1To familiarize students with instrumental methods used in the study of properties of various material
C-2Developing skills of selection of instrumental methods for determining the properties of characterized material
C-3Developing skills to develop research results, their interpretation and use in the characterization of materials
Treści programoweT-L-1Use of magnetochemical methods in the study of substances, such as: qualitative evaluation of magnetic properties, determination of the electronic structure of the central ion
T-L-2The use of spectroscopic techniques in the analysis of the surface - study of the chemical composition of the surface materials by XPS
T-L-3NMR methods used in the studies of organic compounds (preparation of the samples for measurement, the identification of selected compounds on the basis of a series of spectra 1D (1H, 13C, NOE) and 2D (HMQC, HMBC, COSY, NOESY)
T-L-4The use of chromatographic methods in the trace analysis (refering to the analytical system GC/MS, and the system capabilities in qualitative and quantitative analysis on the example of the analysis of petrochemical products, selection of analysis conditions, use a library of mass spectra to identify the analytes)
T-L-5Using x-ray fluorescence spectrometry methods for the analysis of the chemical composition of the materials, such as: determination of promoters (CaO, Al2O3), iron catalyst by standard addition method
T-L-6The use of TG-MS method to the analysis of materials, for example decomposition of the mixture NH4HCO3 and CaCO3
T-L-7The use of X-ray diffraction studies of solids (construction and operation of X-ray diffractometer, qualitative and quantitative analysis of phase composition, determination of medium-sized crystallites and grains of the materials
T-L-8Determining the particle size with DLS technique
Metody nauczaniaM-1laboratory
M-2consultations
Sposób ocenyS-1Ocena formująca: participation in laboratories
S-2Ocena formująca: performing the report
S-3Ocena formująca: written grade
Kryteria ocenyOcenaKryterium oceny
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student knows several research methods used to determine various properties of materials and partly explains the principle of operation of the apparatus
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaChE_3-_B04_W02Student knows the research methods used to determine the various properties of materials and explains the principle of operation used equipment
Odniesienie do efektów kształcenia dla dyscyplinyChE_3-_W04She/he has advanced knowledge of techniques and methods to identify and characterize chemical products.
Cel przedmiotuC-2Developing skills of selection of instrumental methods for determining the properties of characterized material
Metody nauczaniaM-2consultations
Kryteria ocenyOcenaKryterium oceny
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student knows several research methods used to determine various properties of materials and partly explains the principle of operation of the apparatus used
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaChE_3-_B04_U01Student can suggest a suitable test method for determination of the properties of the materials and indicate the possibility of using the obtained results
Odniesienie do efektów kształcenia dla dyscyplinyChE_3-_U10She/he is able to assess the usefulness and ability to use new technological studies and research methods in terms of the direction of research.
ChE_3-_U08She/he is able to use analytical methods and experimental research to solve problems in the field of chemical technology or chemical engineering, especially in terms of the direction of research.
Cel przedmiotuC-2Developing skills of selection of instrumental methods for determining the properties of characterized material
C-3Developing skills to develop research results, their interpretation and use in the characterization of materials
Treści programoweT-L-1Use of magnetochemical methods in the study of substances, such as: qualitative evaluation of magnetic properties, determination of the electronic structure of the central ion
T-L-2The use of spectroscopic techniques in the analysis of the surface - study of the chemical composition of the surface materials by XPS
T-L-3NMR methods used in the studies of organic compounds (preparation of the samples for measurement, the identification of selected compounds on the basis of a series of spectra 1D (1H, 13C, NOE) and 2D (HMQC, HMBC, COSY, NOESY)
T-L-4The use of chromatographic methods in the trace analysis (refering to the analytical system GC/MS, and the system capabilities in qualitative and quantitative analysis on the example of the analysis of petrochemical products, selection of analysis conditions, use a library of mass spectra to identify the analytes)
T-L-5Using x-ray fluorescence spectrometry methods for the analysis of the chemical composition of the materials, such as: determination of promoters (CaO, Al2O3), iron catalyst by standard addition method
T-L-6The use of TG-MS method to the analysis of materials, for example decomposition of the mixture NH4HCO3 and CaCO3
T-L-7The use of X-ray diffraction studies of solids (construction and operation of X-ray diffractometer, qualitative and quantitative analysis of phase composition, determination of medium-sized crystallites and grains of the materials
T-L-8Determining the particle size with DLS technique
Metody nauczaniaM-1laboratory
M-2consultations
Sposób ocenyS-1Ocena formująca: participation in laboratories
S-2Ocena formująca: performing the report
S-3Ocena formująca: written grade
Kryteria ocenyOcenaKryterium oceny
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student can suggest a suitable test method to determine the properties of materials
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaChE_3-_B04_K01Student is open to the knowledge improvement in the field of innovation and to transfer its skills to the others
Odniesienie do efektów kształcenia dla dyscyplinyChE_3-_K01She/he is able to think and act in an innovative, creative and enterprising way.
Cel przedmiotuC-1To familiarize students with instrumental methods used in the study of properties of various material
C-2Developing skills of selection of instrumental methods for determining the properties of characterized material
C-3Developing skills to develop research results, their interpretation and use in the characterization of materials
Treści programoweT-L-1Use of magnetochemical methods in the study of substances, such as: qualitative evaluation of magnetic properties, determination of the electronic structure of the central ion
T-L-2The use of spectroscopic techniques in the analysis of the surface - study of the chemical composition of the surface materials by XPS
T-L-3NMR methods used in the studies of organic compounds (preparation of the samples for measurement, the identification of selected compounds on the basis of a series of spectra 1D (1H, 13C, NOE) and 2D (HMQC, HMBC, COSY, NOESY)
T-L-4The use of chromatographic methods in the trace analysis (refering to the analytical system GC/MS, and the system capabilities in qualitative and quantitative analysis on the example of the analysis of petrochemical products, selection of analysis conditions, use a library of mass spectra to identify the analytes)
T-L-5Using x-ray fluorescence spectrometry methods for the analysis of the chemical composition of the materials, such as: determination of promoters (CaO, Al2O3), iron catalyst by standard addition method
T-L-6The use of TG-MS method to the analysis of materials, for example decomposition of the mixture NH4HCO3 and CaCO3
T-L-7The use of X-ray diffraction studies of solids (construction and operation of X-ray diffractometer, qualitative and quantitative analysis of phase composition, determination of medium-sized crystallites and grains of the materials
T-L-8Determining the particle size with DLS technique
Metody nauczaniaM-1laboratory
M-2consultations
Sposób ocenyS-1Ocena formująca: participation in laboratories
S-2Ocena formująca: performing the report
S-3Ocena formująca: written grade
Kryteria ocenyOcenaKryterium oceny
2,0Student does not meet the criteria for the assessment of 3,0
3,0Student is open to a limited extent to the knowledge improvement in the field of innovation and to transfer its skills to the others
3,5
4,0
4,5
5,0